The TGA body weight adjust curve is revealed in Determine one. The main weightloss phase is the volatilization accompanied by a major decomposition phase. The spinoff of body weight transform curve in inexperienced reveals a peak where the height max is at 427.seventy one ˚C. The MS details is gathered through the overall TGA experiment. Ion currents and TGA mass reduction are plotted for a perform of temperature (see Figure 2). It's important to bear in mind the merchandise of the TGA exam are Commonly decomposition products and solutions, and that's genuine in these experiments at the same time. Consequently, the goal is to comprehend the thermal degradation goods of nylon sixty six. TGA-MS continually displays the decomposition off gases for a perform of time and temperature. The degradation mechanism in the polymer molecules breaking for the C-N bond generates smaller sized polymer molecules While using the very same unit of bicarbonyl polymethylene fragments as well as fragments will stop working into carbon dioxide, carbon monoxide, water, and hydrocarbons [five].
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TGA-FTIR consistently monitors the decomposition off gases like a perform of your time and temperature, even though GC/MS can separate the several off-gasoline products that arrive off at just one stage in time.
The degradation of nylon 66 On this part of the examine was also completed on a TGA5500. The off-gas products ended up analyzed using a FTIR to the IR spectra along with a GC/MS with the MS analysis.